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Plastic Biodegradability Test (ISO 14855-1, 2)

For the evaluation of plastic biodegradability, various testing methods have been established in international standards such as ISO, JIS, ASTM, and others. Here, I will provide an example of a testing method.

Plastic Biodegradability Evaluation Test

tandard NumberISO 14855-1(JIS K 6953-1、ASTM D5338)ISO 14855-2(JIS K 6953-2)
Standard Title

Plastics – Determination of the Ultimate Aerobic Biodegradability under Controlled Composting Conditions – Method by Measurement of Evolved Carbon Dioxide

Part 1: General Method

Plastics – Determination of the Ultimate Aerobic Biodegradability under Controlled Composting Conditions – Method by Measurement of Evolved Carbon Dioxide

Part 2: Mass Measurement Method of Evolved Carbon Dioxide in Laboratory-Scale

OverviewMeasurement of Biodegradability in the Presence of Oxygen
by Microorganisms in Compost
Seeding SourceCompost
The shape of the test samplesGranular, Powdery, Film, and Molded products (testing conducted with the maximum surface area adjusted to approximately 2 square centimeters).Granular, Powdery, Film
Test Container2 liters to 5 liters (can be used for screening purposes in quantities less than 2 liters).250 mL
Test Temperature58±2°C (Can be conducted at any temperature if the sample’s melting point is low)58±2℃
Test Period~6 months
(The duration can be shortened if a steady state is reached, and it can be extended if significant biodegradation is occurring)
MeasurementCarbon dioxide evolution
Evaluation

Biodegradability (%)
[Calculation Formula]
Biodegradability (%) = (CO₂ evolution from the sample – CO₂ evolution from the blank) / Theoretical CO₂ evolution × 100
※ Theoretical CO₂ evolution = Sample weight × Carbon content × (44/12)
Example: For PLA (without additives), with a molecular weight of 72 and a carbon content of 36 (resulting in a carbon content ratio of 0.5). Therefore, the theoretical CO₂ evolution from 10g of PLA is 10g × 0.5 × (44/12) = 18.3g.
※ In cases where the sample is not a single material (contains additives, etc.), and calculating the theoretical CO₂ evolution is challenging, the Total Organic Carbon (TOC) value is necessary.

CO2 Concentration Measurement Device – ISO 14855-2

Biodegradation Apparatus – ISO 14855-2

Our organization undertakes commissioned tests for the biodegradability evaluation of plastics. Additionally, we are entrusted with chemical analysis tests related to the identification criteria (biodegradable plastic, biomass plastic) established by the “Japan Bioplastics Association,” covering specific elements and specific harmful substances.

“Biodegradable Plastic” mark of Japan BioPlastics Association (JBPA)

BOKEN is a certified testing institution of JBPA

Our organization is registered as a testing institution for conducting tests required for inclusion in the Positive List (PL) of the identification labeling system operated by the Japan Bioplastics Association (JBPA)
(see photo on the right: JBPA Certified Testing Institution Certificate).

Therefore, we are capable of conducting biodegradability tests [ISO 14855-2 (JIS K 6953-2)] for obtaining the “Biodegradable Plastic” mark.